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Artigo Científico | Síntese de Materiais Cerâmicos | Inglês | 30/04/1999

Influence of Process Conditions on Hydroxyapatite Crystallinity Obtained by Direct Crystallization

Autores: J.V. Valarelli, M. Danese, M. Giulietti, M.M. Seckler, R. Rodríguez-Clemente, S. Derenzo

Palavras-chave: bioceramic, biomaterial crystallization precipitation, hydroxyapatite

Resumo: Crystallization from solutions was applied to produce stoichiometric and crystalline hydroxyapatite (HAP) suitable for use as a biomaterial. This was accomplished by keeping a low supersaturation through the following procedure: semi-continuous operating mode, slow reactant addition rate and addition of a calcium complexing agent. A high temperature (90 °C) and probably carbonate incorporation also favored the formation of a well crystallized material. A qualitative correlation was found between the supersaturation and HAP properties such as crystallinity and particle size.

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Materials Research

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